An Efficient and Solvent Free Synthesis of N-Aryl 2, 3-Dihydro-4H Naphtho-[2, 1-E] 1, 3-Oxazines

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Year:
2020
Type of Publication:
Article
Keywords:
Aryl, 1, 3-Naphthoxazines, Solvent Free and Synthesis
Authors:
Mohammad S. Al-Ajely; Ahmed M. Noori
Journal:
IJISM
Volume:
8
Number:
4
Pages:
173-182
Month:
July
ISSN:
2347-9051
Abstract:
Oxazine compounds have proved to have many pharmaceutical applications and most of these compounds now a days are used as drugs. For the importance of this class of heterocyclic compounds we are here investigate the synthesis of new derivatives of 1,3-oxazines using solvent free one pot three component system in a drug discovery program, so starting from β-Naphthol, formaldehyde and aromatic amines in presence of zarconyl chloride as catalyst. Compounds 1-9 were synthesized, Benzo 1,3 diazines(10-14) were also synthesized from their corresponding 1,3 oxazines. These compounds were characterized by IR, some representative by 1HNMR and were discussed.

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